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刊物信息

期刊名称:药物分析杂志
主管单位:中国科学技术协会
主办单位:中国药学会
承办:中国食品药品检定研究院
主编:金少鸿
地址:北京天坛西里2号
邮政编码:100050
电话:010-67012819,67058427
电子邮箱:ywfx@nicpbp.org.cn
国际标准刊号:ISSN 0254-1793
国内统一刊号:CN 11-2224/R
邮发代号:2-237
 

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50批不同来源白术药材及饮片中白术内酯Ⅰ和白术内酯Ⅲ含量的HPLC法测定

HPLC determination of atractylenolide Ⅰ and atractylenolide Ⅲ in 50 batches crude drugs and slices of Atractylodes macrocephala Koidz. from different sources

作者: 刘玉强, 才谦 
作者(英文):LIU Yu-qiang, CAI Qian
分类号:
出版年·卷·期(页码):2012,32 (7):0-0
DOI: 10.16155/j.0254-1793.2017.01.01
-----摘要:-------------------------------------------------------------------------------------------

目的: 采用HPLC法测定不同来源白术药材及饮片中白术内酯Ⅰ和白术内酯Ⅲ的含量。 方法: 采用Tigerkin C18(5 μm,4.6 mm×250 mm)色谱柱,流动相为甲醇-水(67: 33);流速为0.8 mL·min;检测波长为220 nm;柱温30℃。 结果: 10批市售白术药材和40批市售白术片及麸炒白术片中白术内酯Ⅰ和白术内酯Ⅲ含量差别均较大。 结论: 不同来源市售白术药材及其饮片质量差别较大。

-----英文摘要:---------------------------------------------------------------------------------------

Objective: To determine the contents of atractylenolide Ⅰ and atractylenolide Ⅲ in crude drugs and slices of Atractylodes macrocephala from different sources by HPLC. Methods: The samples were separated on Tigerkin C18 column(5 μm,4.6 mm×250 mm)with the mobile phase of methanol-water(67: 33)at the flow rate of 0.8 mL·min-1.The detection wavelength was set at 220 nm,and the column temperature was 30℃. Results: The contents of atractylenolide Ⅰ and atractylenolide Ⅲ in 10 batches crude drugs and 40 batches slices of Atractylodes macrocephala were relatively large differences. Conclusion: The quality of Atractylodes macrocephala from different sources were different.

-----参考文献:---------------------------------------------------------------------------------------
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7 NAN Yang(南洋),JIA Ling-yun(贾凌云),LI Qian(李倩),et al.RP- HPLC simultaneous determination of atractylodin and atractylenolide Ⅱ in Rhizoma Atractylodis(RP-HPLC法同时测定苍术中苍术素和白术内酯Ⅱ的含量).Chin J Pharm Anal(药物分析杂志),2010,30(1):17
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9 PENG Teng(彭腾),JIA Bo(贾波),ZHANG Xu(张旭),et al.Determination of atractylenolide Ⅲ in Atractylodes Poria soup with different ratios by HPLC(HPLC法测定白术茯苓汤不同配比水煎液中的白术内酯Ⅲ).West China J Pharm Sci(华西药学杂志),2010,25(1):57
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11 LIU Yu-qiang(刘玉强),ZHEN Bi-xian(甄毕贤),CAI Qian(才谦),et al.Determination of atractylenolide Ⅱ in crude drugs and slices of Atractylodes macrocephala Koidz.from different areas by HPLC(不同地区白术药材及饮片中白术内酯Ⅱ的含量测定).Chin J Exp Tradit Med Form(中国实验方剂学杂志),2012,18(4):120

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